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フッ素分離における拡散条件の検討
https://mdu.repo.nii.ac.jp/records/417
https://mdu.repo.nii.ac.jp/records/4170fa851ec-f671-44d1-b620-dff896f970f7
名前 / ファイル | ライセンス | アクション |
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Item type | Journal Article(1) | |||||||
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公開日 | 2012-05-24 | |||||||
タイトル | ||||||||
タイトル | フッ素分離における拡散条件の検討 | |||||||
言語 | ||||||||
言語 | jpn | |||||||
資源タイプ | ||||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||||
資源タイプ | journal article | |||||||
その他(別言語等)のタイトル | ||||||||
その他のタイトル | Studies on Separation of Fluoride using Diffusion Method | |||||||
著者 |
上条, 啓子
× 上条, 啓子
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抄録 | ||||||||
内容記述タイプ | Abstract | |||||||
内容記述 | Separation is necessary to the determination of fluoride in most types of biological samples except bone and teeth. At present, the diffusion procedures have widely used because many samples can be dealt with at one time and high temperatures are not required. In 1967 D. R. Taves discovered that diffusion of fluoride was greatly accelerated by the presence of silicone grease containing acidified sample and led to the development of a new procedure for rapid diffusion of fluoride at room temperature, using hexamethyldisiloxane (HMDS). Consequently, we studied several conditions concerning acidified samples containing HMDS in diffusion. Diffusion bottle on the market (Tupper Ware Minicup) was used and filter paper (12×25 mm) was hanged for trapping of fluoride. The results of several experiments are summarrized as follows: 1. As trapping solution 0.5 M sodium hydroxide was effective in fluoride recovery rate compared with 0.5 M magnesium succinate. 2. The concentration of perchloric acid for evolution of fluoride ranging 2.7 to 2.7×10^<-2>M makes no difference in recovery of fluoride. 3. HMDS in sample solution shortened the diffusion time. In addition to that, shaking of diffusion bottle shortened the diffusion time up to 30 to 60 minutes at room temperature. | |||||||
書誌情報 |
松本歯学 巻 4, 号 2, p. 150-153, 発行日 1978-12-31 |
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出版者 | ||||||||
出版者 | 松本歯科大学学会 | |||||||
ISSN | ||||||||
収録物識別子タイプ | ISSN | |||||||
収録物識別子 | 0385-1613 | |||||||
書誌レコードID | ||||||||
収録物識別子タイプ | NCID | |||||||
収録物識別子 | AN00232590 | |||||||
フォーマット | ||||||||
内容記述タイプ | Other | |||||||
内容記述 | application/pdf | |||||||
著者版フラグ | ||||||||
出版タイプ | VoR | |||||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 |